Publication

The effect of titania precursor on the morphology of prepared TiO2/MWCNT nanocomposite materials

László Forró, Arnaud Magrez, Endre Horvath, Klara Hernadi
2014
Journal Articles

Abstract

Since materials science is of great importance, the application of composite materials based on carbon nanotubes (CNTs) is widely investigated. Current work is aimed at preparing nanocomposites of TiO2/MWCNT using an impregnation method combined with slow hydrolysis. Different titanium alkoxide compounds as Ti(OEt)(4), Ti(OiPr)(4), and Ti(OBu)(4), respectively, were used as precursor materials to cover the surface of CNTs in ethanolic medium. In our samples themass ratiowas 10:1 (TiO2:MWCNT). The produced composite materials were characterized by X-ray diffraction (XRD), energy-dispersive X-ray spectroscopy (EDX), Raman microscopy, transmission (TEM) and scanning electron microscopy (SEM) techniques; moreover, thermal analysis and the determination of the specific surface area (BET) were also carried out. These as-prepared TiO2/MWCNT composites were also tested as photocatalysts in degradation reaction of the model compound salicylic acid. (C) 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim

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https://infoscience.epfl.ch/entities/publication/18da4b32-f67a-4b19-900d-301df3336f7d

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László Forró, Arnaud Magrez, Endre Horvath, Klara Hernadi
2014
Journal Articles

Abstract

Official source

https://infoscience.epfl.ch/entities/publication/18da4b32-f67a-4b19-900d-301df3336f7d

About this result

Related concepts (29)

X-ray spectroscopy

X-ray spectroscopy is a general term for several spectroscopic techniques for characterization of materials by using x-ray radiation. When an electron from the inner shell of an atom is excited by the energy of a photon, it moves to a higher energy level. When it returns to the low energy level, the energy which it previously gained by the excitation is emitted as a photon which has a wavelength that is characteristic for the element (there could be several characteristic wavelengths per element).

Scanning electron microscope

A scanning electron microscope (SEM) is a type of electron microscope that produces images of a sample by scanning the surface with a focused beam of electrons. The electrons interact with atoms in the sample, producing various signals that contain information about the surface topography and composition of the sample. The electron beam is scanned in a raster scan pattern, and the position of the beam is combined with the intensity of the detected signal to produce an image.

Titanium dioxide

Titanium dioxide, also known as titanium(IV) oxide or titania taɪˈteɪniə, is the inorganic compound with the chemical formula TiO2. When used as a pigment, it is called titanium white, Pigment White 6 (PW6), or CI 77891. It is a white solid that is insoluble in water, although mineral forms can appear black. As a pigment, it has a wide range of applications, including paint, sunscreen, and food coloring. When used as a food coloring, it has E number E171. World production in 2014 exceeded 9 million tonnes.

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